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Table 3 Synthesis of pyrazole 11a–l under both ultrasonic irradiation and conventional method

From: Ultrasonic irradiation assisted efficient regioselective synthesis of CF3-containing pyrazoles catalyzed by Cu(OTf)2/Et3N

Compound no.

Product

Ultrasonic irradiation

Silent condition

  

Time (min.)

Yield%

Time (h)

Yield%

11a

45

90

7

80

11b

45

88

7

76

11c

45

90

6

77

11d

45

88

8

75

11e

45

88

10

76

11f

45

85

10

76

11g

60

89

10

76

11h

60

90

10

77

11i

60

85

11

73

11j

60

85

11

77

11k

60

86

9

75

11l

60

90

10

77